Appearance White to off-white crystal or flake crystal
Assay 98%min
Identification Positive
Melting point 147-150℃
Loss on drying 1.0% max
Acidity 0.5ml max
Residue on ignition 0.2% max
Mould 100/g max
Total bacteria 1000/g max
Appearance White Powder Or Free-Flowing Granules;
Solubility Slightly in alcohol, easily in water
Identification The Infrared Absorption Spectrum Of The Preparation Of The Test Specimen Exhibits Max Only At The Same Wvelength As That Of A Similar Preparation Of The Corresponding Usp Ref. Standard
Conductivity Not more than 20μS • cm-1
Clarity
Appearance Colorless, transparent liquid
Assay 99%min
Relative density 1.017-1.020
Refractive index 1.5290-1.5350
As content 0.0001% max
Heay metals(as Pb) 0.0001% max
Appearance White crystalline powder
Assay(as C4H7Cl3O.1/2H2O) 98.5%min
Melting point 76-78℃
Residue on ignition(as sulfate) 0.1% max
Chloride 0.005% max
Solution in ethanol Pass
Acidity Pass
Appearance White crystalline powder, odorless
Identification IR: Concordant with R.S
HPLC: TR Concordant with R.S
Specific rotation -49.0°~-55.0°
Related substance 2.0% max
Microbial limits Concordant with R.S
Bacterial endotoxins Concordant with R.S
Loss on drying 1.0% max
Residue on ignition 0.2%max
metals 20ppm max
Assay(HPLC) 97.0-102.0